Method of and means for obtaining and measuring gaseous samples



June 20, 1944. H, u. JARRETT METHOD OF AND MEANS FOR OBTAINING AND MEASURING GASEOUS SAMPLES 2 Sheets-Sheet 1 Filed May 12, 1941 Hen June 20, 1944. U, JARRETT 2,351,764

METHOD 0F AND MEANS FOR OBTAINING AND MEASURING GAsEoUs SAMPLES Filed May 12, 1941 2 Sheets-Sheet 2 ZIN Patented June 20, 1944 MEANs-oa on'rsmmd MEASURING GAsEoUssAMPLEs Henry U. Jarrett, Palestine, Tex.,"assignor o f'one- ,y

, half to W; 0. Whiteside, Lo'ligviewdlex.

This invention relates to new and useful irn-y vcharged from al well under normal' owing condi,-

tions and accurately. measuring the liquid and/or liqueiiable hydrocarbon content of said sample to determine the gas/oil ratio thereof.

Another object of the invention is to provide an improved fluid sampling method which includes the preliminary step of settling out the hydrocarbons whichare liqueed or readily liqueable prior to the conventional measurement of the liqueilable-hylrocarbon content ofthe sample, whereby a more accurate measurement is obtained.

A particular object of the invention is to provide an improved method,fof the character described, wherein the pressure of the well iiuids is utilized as the operating medium for 'actuating the sample obtaining means.

A further object of the invention is to provide an improved uid sampling method which includes separating the liquefied or readily liqueable hydrocarbons from the fluid sample, then passing said fluid sample through an absorbent to separate the liqueable hydrocarbons from the non-liquefiable hydrocarbons, the preliminary separation of such hydrocarbons resulting in the prevention of excessive saturation of the absorbent and the consequent loss of said hydrocarbons due to the excessiveness of the saturation, whereby the percentage of liqueiiable hydrocarbons present, in the sample may be more accurately ascertained.

Still another object of the invention is to provide improved fluid sampling means which is adapted to be actuated solely by the energy of the well fiuid pressure within the well being tested and which is adapted to be readily moved from well to well, whereby elimination of auxiliary operating means and a considerable saving of time are eiected not only in running the tests but also in the installation and removal-of the sampling means.

A still further object of the invention is to provide an improved apparatus for obtaining and testing fluid samples from a flowing well which includes a pressure-responsivemember adaptedtobe actuated by thepressure-y of the well fluids for operating the huid-sampling tube and which also includes av separator or trapping the liquids in suspension to prevent undue saturationof the absorbent employed in measuring the percentage of liqueable hydrocarbons present in the huid samples, whereby an emcient and economical measurement of the gas and Oil ratio is had. l

The construction designed to carry out the invention will be hereinafter `describedtogether with other features of the invention.

The invention will be more readily understood from a reading of the following specification and by .reference to the accompanying drawings, as an example of the invention `is shown, and wherein: y I f y Figure 1 is a view, partly in elevation and partlyL in section, V`of an apparatus constructed in accordance with the invention and mounted upon the iiow connections of a well,

Figure 2 is an enlarged, transverse, vertical sectional view of the upper portion of the apparatus, f

Figure 3 is a view, similar to Figure 2, of the lower portion ofthe apparatus, f

Figure 4 is a horizontal, cross-sectional view, taken on the line 4-4 of Figure 1,

Figure 5 is a horizontal, cross-sectional view, taken on the line 5-5 of Figure 2,

Figure 6 is a schematic view of one, of the twoway valves, and A Figure '7 is a view, .similar to Figure 6, of the valve in its opposite or reverse position.

In the drawings, the numeral I0 designates a well casing having the usual casing head II mounted on its upper-end for supporting a well tubing I2 axially within the same. A ow connection or cross I3 is disposed above the casing head, while a gate valve I4 is interposed between the cross and the casing head. 'I'he ow cross communicates with the bore of the tub-- ing I2 and has the customary iiow pipes I5-connected in its lateral outlet ports I6. 'The above elements constitute the conventional hook-up or control assembly of a flowing well and form no part of the present invention.

A uid sampling apparatus A is adapted to be mounted above the ow cross I3 and includes an elongate, cylindrical body or member I1 having an axial bore I8 formed in its upper end. A tubular sleeve I9., having an 'internal diameter substantially equal to the diameter of the bore I8, is screw-threaded into the upper endof the body I1 so as to provide an elongate cylinder 28, the upper end of which is closed by a cap member 2l. An .axial counterbore 22` is disposed within the lower portion of the body I1 below and in communication with the bore I8 and has its extreme upper end enlarged to provide an annular recess or chamber 23. The lower portion of the counterbore is also enlarged to form a stumng box or packing chamber 24 for receiving a cylindrical packing member 2l, oi' rubber, Neoprene or other suitable resilient material, which is conilned therein by a screwthreaded gland or follower 28. An externally screw-threaded nipple 21 depends axially from the lower end of the body I1 and is threaded within the upper end oi' al box 28, thebore `28 of which has its lower end reduced to provide a counterbore 38. The joint between the `Vabutting surfaces of the body and box is preferabl .sealedofl by a suitable packing ring 3|.

For detachably connecting the sampling apparatus A to the flow cross I3, the'lower end 32 of the box 28 is reduced and externally screwthreaded, whereby it may be readily connected with a suitable coupling collar 33 which is fastened by a nipple or short sleeve 34 to the upstanding'ilange oi' said flow cross. A lateral, screw-threaded port or opening 38 (Figure 3), arranged to receive the lower endof a pipe or tube 38 which extends longitudinally andv externally of the apparatus A, is formed in the wall of the box 28; The upper end of the pipe 36 is screwthreaded within a similar port 31. provided in the side wall of the cap member 2 I, whereby said pipe establishes communication between the upper end of the cylinder 20 and the bore 28 of the box. Suitable manual control valves 38 and 39 are mounted in the pipe 38, `one valve being disposed adjacent the port 35 and the other valve'positioned intermediate the ends of said pipe. Be-

- bore of the packing gland nu't 28,

y control valves 38 tween the lower valve 38 and the upper valve 33,

the pipe communicates or chamber 23 of the body I1 by means of a twoway valve 4I extending laterally through the wall oi.'r said body. 'When-the valve 40 is in one position as shown lin Figure 6, communication is established between the lower portion of the pipe 38 and the recess 23 and shuts oil! the upper portion of said pipe. In its other position, the valve 48 closes the port 4I ,and permits the lower portion of the pipe to4 communicate with the upper portion thereof (Figure 7). A similar two-way valve 42 is mounted in the pipe 38 above the valve 39 and has its third branch communicating with the atmosphere, whereby the upper portion of said pipe `may be brought into communication with the lower portion thereof or with the atmosphere. Diametrically opposite the port 4I which opens into the annular recess ,23, a complementary port or outlet opening `43 is provided and is arranged.

to receive a suitableoontrol valve 44.

with the annular recess 48 which is screw-threaded in a port of the bore 48 and an annular groove or recess 48, formed in the exterior of the piston at its intermediate portion, is established by a radial duct 38 (Figure 4).` As shown in Figure 1, the tube 41 is of sufllcient length to extend below the flow connection of the casing head when the piston is in its lowerxnost position. enlarged hollow tip or head II, having its lower, external surface bevelled to provide an annular knife-edge 52 on its lower end, is screw-threaded on the lower extremity of the tube. The external dimeter of the tube is substantially equal to the diameters of the bore 22 of the body I1 and the whereby said tube has a snug sliding llt within said bores and has its external surface sealed oil.' by the packing member 28. The tube also extends axially through the bore 28 and counterbore 38 of the box 28, the counterbore being of a slightly greater diameter than said tube so as to provide an annular flow space exteriorly of the tube between the bore of the well tubing and said bore 28. When the tube and piston are in their lowermost positions, the external annular groove 48 o1' said piston is in registration and communicats with a discharge opening or port 53 formed in the cylinder wall as shown in Figure 1.

Prior to the connection oi' the sampling apparatus A tothe flow cross I3, the piston v45 and tube 41 are preferably in their uppermost positions with the upper end of said piston engaging the upper stop formed by the cap member 2| and the tip 8| of said tube is in close proximity to the lower end of the box 28. After coupling the apparatus to the ilow cross, the gate valve I4 and and 38 are opened to permit ow from the tubing, through the counterbore 38 and bore 29 of the box' 28, through the pipe 38 and then4 into the upper end of the cylinder 28, whereby the pressure of said well fluids may be exerted against the upper end of the piston. At this time, the valves 48 and 42 are in a position establishing communication therethrough and are closed off from the port 4I and atmosphere, respectively (Figure 7),v while the valve 44 is preferably opened to permit the escape of any pressure trapped within the cylinder below the piston. The pressure of the well the well fluids to A- piston or plunger 45, having a plurality of sealing rings 46 mounted in grooves on its vexternal surface, is slidably disposed within the cylinder 28 and has an elongate, cylindrical sampling tube 41 depending axially therefrom. Due to the provision of the recess 23 and cap member 2| which form' internal, annular shoulders at the fends of the cylinder, upper and lower stops for the piston 45 are provided. The tube 41 is preferably screwthreaded into the lower end of the piston 45 and communicates with a small axial bore 48 formed within the lower portion of said piston. Communication between the upper end ton will force' said piston and the tube downwardly until the lower end of the piston strikes the lower stop or shoulder of the cylinder. When -the piston and tube have reached their lowermost positions, it is preferable to close the valves 38 and 44 as the pressure of the well fluids trapped within the cylinder above said piston is sufficient to maintain the same in such position. With the piston in this position, the lower end of the tube will be below the connection of the casing head II as well as a considerable distance below the outlet ports l5 of the flow cross as shown in Figure 1. Also, the annular groove 49 of the piston will be in registration with the discharge opening 53, whereby fluid entering the bore of the tube will be conducted through the bore 48 and duct 58 of said piston into said groove and outwardly through said opening,

To elevate the piston and tube, the Valve 38 is again opened and the valves 48 and 42 are moved to their non-communicating or second positions (Figure 6) so as to communicate with the port 4I and atmosphere, respectively. Thus, the well fluids within the pipe 36 will be conducted by the valve 48, port 4I and recess 23 to the lower end of the cylinder. Since the upper portion of the the ydischarge opening into an laxial i opening recting the well sampling tube 41, piston bore a Pipe, 36 isin communication with the atmosphere "due tothe position ofthfyaive 42'the weliflurids withinfth'ef,-

dr-.awveihal bision ae eX- rmit the f ree' Iupwardjmovement of sample Noij the ,wll` fluids or untily lthe apparatus is' removed tofanother' well... In thelatter event,

the gate valve I4'is`closed prior to Adisconnection and the va1ve-44 is opened' to permit the escape of the weil fluids trapped withiny thecylinder belowthe piston'.l f

For determining the liqueflable hydrocarbon content` or gas/oil ratio of'a sample of the Well fluids, anabsorption tube 54 communicates with 53 of the cylinder `by means'of 'pipesvor conductors'55 and 56.` The tube 54 is yfilled with charcoal. or any other suitable absorbent, and has its lower or outer end 'connected by a pipe 51 to a suitable meter (not shown) whereby the volume or quantity of the liquefiable hydrocarbons of 'the' well .iluid sample may be measured. The pipe 56is connected to the opening 53'by a manual control vvalve 58 screw-threaded into said opening, said pipe preferably extending longitudinally of the body l1 and sleeve I9 and upwardly from said opening. Interposed between the adjacent ends of the pipes 5 and 56 and establishing communication therebetween is lan upright, cylindrical tank or housing 59 having its top and bottom ends curved or rounded as designated by the numeral 66. A manual controlvalve k6I is screw-threaded 62 formed in the bottom of the housing.` while a complementary opening 631s provided in the top of said housing for re ceiving the upper or free end of the pipe 56. Communication between the pipe 55 and the interior of the housing 59 is provided by the upper end of said pipe engaging within a port 64 formed in the sidewall of said housing adjacent its top. The pipe 55 preferably depends lfrom the port "tubef The 'valve 36isthen 'closed fil 64 so as to extend longitudinally of the housing and has a suitable hand valve 65 mounted there- As is clearly shown in Figure 2` the interior of the housing is hollow so as to provide a chamber 66 for receiving the well uid sample discharged from the opening 53 of the cylinder 20 into the pipe 56. An arcuate trough 61 is disposed adjacent the port 64 for preventing the entrained liquids or readily liquefiable hydrocarbons of the sample from flowing through said port into the pipe and absorption tube 54 and is preferably made integral with the inner surface of the chamber wall (Figure 5). For difiuid sample asA it enters the chamber 66 to the intermediate portion thereof, a short, tubular sleeve 6R depends axially from the top of the housing to a point below the trough 61 and forms a continuation. of the pipe 56,'

Thus, the well fluid sample, conducted by the groove 49 to the opening 53 of the cylinder 20. will bedischarged` into the intermediate portion of the chamber 66 by the pipe 56 and sleeve 68. Immediately upon entering the chamber, the lighter ends or non-licueed hydrocarbons present in the fluid sample will rise and flow over the wall of the trough 61 into the pipe 55 and absorption tube 54, while the entrained liquids and readily liquefiable hydrocarbons will flow downwardly and settle to the bottom of said chamber by reason of their weight. Due to the bore of the tubing.

4R. duct 50 and enlarged areaY yof. slight.: dropA in th "ofv Portion. er

4bons' will. y .bev` trai) 'arator I for trapping nth ,m

l well fluids into The-remaining, ,liq ds v )fbi/.ih c

absorbent, Withinv the, tub

chamber 66; serves as a entrained liquids, and/,or readily 11al drocarbons," whereby a vsubstantially fluid sample is deliveredto theflabslo i By preventing `the passag'e ofan.; appreciable amount of free ,liquids and/or',readilyy liqueilable hydrocarbons, to the '..absorptiontube, yexcessive saturation of the absorbentand;by-pass,of said Vliquids and/or hydrocarbons throughsaid tube is eliminated. f n, From the foregoing'it is lobviousthegas/ol ratio or liqueilable. hydrocarbon content ofthe well fluid sample. may be readily ascertained by combining the liquids and/orliquefied hydrocarbons trapped in the separating chamber, andabsorption tube and computing the percentage thereof.

When it is desired to obtainand measure a representative vwell fluid sample or samples, the sampling apparatus A is connected to the flow crossv I3 ofthe Well with thepiston 45 andvtube 41 in their uppermost positions 4(Figure 2). has been hereinbefore fully described, the valves 3B. 4 0, 39 and 42 are then manipulatedso as to establish communication between the bore 2 9 of the box 28 and the upper end of the cylinder 20 by means of the pipe 36,` whilethe valvev 44 is opened to exhaust any pressuretrapped withinsaid cylinder below the piston. livitlrtlieelements in the above position. the pressure' of the well fluids will be exerted against theupper end of ythe piston and will force the same downwardly until its lower end engages the lower stop of the cylinder, whereby the yannular groovev49 of said piston will be moved into registration with the discharge opening 53 and the tip '5| of the sarnpling tube will kbe disposed below the ow yconnecticn of the casing headli. T he valves 38 and 44 are then closed and the valves 58 and 65 opened to permit the well fluids to flow from the through the sampling tube, into the chamber 66 of the separator 59 and the absorption tube 54. Due to the provisionof the annular knife-edge 52 of the tip 5| and the positioning of the same below the flow connections of the well control assembly,there is a substantially uninterrupted, representative flow of the the sampling tube. After a suitable sample of the well fluids has been obtained. the valve 58 is closed to shut 01T the flow thereof to the separator 59.

I'he liquids trapped within the absorption tube 54 and the chamber 66 of the separator are then removed and combined sothat ythe percentage thereof relative to the volume of the sample may be computed. In removing the liquids from the separator chamber, the valve 6I is opened to permit the same to drain therefrom Duey to the passage of ther gaseous fluids and lighter hydrocarbons from `the chamber iinto the absorption tube after the'closingof the valve 58. the liquids within said' chamber will be unthereabove, whereby said` chamber 66 and the absorption I 5|' of the tube ',be moved to' another `within the scope of l hydrocarbon liquids will rise within said chamber and tend to now intothe trough B1 and out,v through the port 6I. To overcome this dilculty, the sleeve 08 has been extended a sumcient distance below the trough to break up the agitationI of the liquids so that the same will only rise to a predetermined point. Thus, the sleeve serves the two-fold purpose of directing the well nuids'to the interme- 'diatev portion of the chamber and preventing un- `the escape of the trappedv or `ing communication between the bore 2K9 of the box 28 and the lower endof thecylinder and y permitting the well fluids trapped in said cylinder having a flow control above the piston to escape to atmosphere. `Since f the pressure of the well fluids is exerted against kthe llower end oi' the piston, the same will be raised to its upper position as shown in Figure 2. When the pistonis in this position,the tip 41 will be immediately below the box 28 and thedisconnection of the apparatus may b e accomplished by uncoupling said box from the flow cross I3. The apparatus may then .well or stored for future pressure of the well fluids it is obvious that the necesuse; By utilizing the to actuate the piston,

l vsity of auxiliary operating means for actuating 'the sampling tube is eliminated so as to provide a more economical and emcient mechanism.

The foregoing description of the invention is explanatory thereof and various changes in the size,` shape and materials, as well as in the details of the illustrated construction may be made,

the appended claims, without departing from the spirit of the invention.

What I claim and desire to secure by Letters Patent is:

l. The method of determining the liqueflable content of the fluid discharged from a flowing well which includes, obtaining a representaltive sample of the well fluids from the well bore prior'to the discharge of said fluids, separating the liquefied and readily liquefiable hydrocarbons from the sample, then passing the remainder `of said sample through an absorbent to separate the liqueflable hydrocarbons from the remainder ofthe sample, and then combining the separated liquefied and liqueable hydrocarbons and computing the percentage thereof.

2. An apparatus for obtaining a sample of fluid from a high pressure flowing well and separating its liquefiablel hydrocarbon content including, means' for obtaining a representative well fluid sample from the tubing of a flowing well below theA flow connections thereof, means for settling out the liquefied hydrocarbons from the sample obtained, means for conducting said sample from the obtaining means to the settling means, and

vabsorption means` for receiving the remainder of the sample from said settling means and for vtrapping the liqueflable hydrocarbons therein Vwhereby the recovered hydrocarbons'may be combined and the percentage thereof computed.

3. An apparatus for obtaining a sample of fluid from a high pressure ing its liqueflable hydrocarbon content including, means for obtaining a representative well fluid sample from vthe tubing of a owing well flowing well and separatbelowl the flow connections thereof, a chamber having connection with the obtaining meansv for receiving the sample and settling out liquefled and readily liqueflable hydrocarbons, and an absorption tube communicating with the chamber for receiving the remainder of said sample and trapping the liquei'iable hydrocarbons therein, kwhereby said hydrocarbons maybe recovered from the tube and chamber to permit combining and computation of the percentage thereof.

4. A sampling apparatus for a flowing Well assembly mounted upon with its bore including, a tubular body adapted to be connected to the control assembly with its bore communicating with the bore of the well tubing and having a cylinder formed-therein, the cylinder having a valve-controlledoutlet, a piston member slidably mounted within said' cylinder, a tube depending from the member through the lower end of the cylinder vinto the bore of the body and adapted to be lowered into and raised from the well tubing by said member for receiving a well fluid sample, means for sealing oil between the tube and said body bore to prevent direct communication between said tubing and the cylinder, means for selectively conducting the well fluids to the upper and lower ends of said cylinder whereby the well fluids may be directed to either end of the cylinder to reciprocate the piston member and tube, and meansfor exhausting said well fluids from the upper and lower'ends of said cylinder, said member having a passage therein communicating with said tube and closed oft' by the cylinder wall to prevent escape of the fluid sample, thevpassage of the `member registering with the outlet of said lcylinder only when said member is moved to its lower position forv conducting said sample from said tube to and in communication `said outlet.

ered into and raised yfrom the well tubing by said member for receiving a well fluid sample, means for sealing oil' between the tube and said body bore to preventv direct communication between the cylinder and tubing, means for 4establishing communication between said well tubing and the upper and lower ends of said cylinder, means for controlling the flow of well fluids through the communicating means, whereby the well fluids may be directed to either end of the cylinder to reciprocate said piston member and tube, and means for exhausting said well iluids from the upper and lower endsof said cylinder to assist the reciprocatii n of the member and tube, said member having a passage therein communicating withA said tube and closed off by the cylinder wall to prevent the escape of the fluid 6. A sampling apparatus for a flowing well having a flow control assembly mounted upon and in .communication with its bore including, a. tubular body adapted to be connected to the control assembly so as to communicate with the Well tubing and having a cylinder formed therein, the cylinder having a valve-controlled outlet, a piston member slidably mounted within the cylinder. a tube depending 4from the member and extending through the lower end oi said cylinder into the bore of the body and adapted to be lowered into and raised from the bore of the tubing by said member for receiving a well fluid sample, means for sealing off between the tube and said body bore to prevent direct communication between the cylinder and tubing, a conduit for establishing communication between said tubing and the upper and lower ends of said cylinder, valves for controlling the flow of well fluids through the conduit, whereby the well uids may be directed alternately to the opposite ends of the cylinder to reciprocate the piston member so as to raise and lower the tube, and means for releasing said well iiuids from the upper and lower ends of the cylinder, said member having a passage therein communicating with said tube and closed off by the wall of said cylinder to prevent the iiuid sample from escaping, the passage of the member registering with the outlet of the cylinder only when said member is moved to its lower position for conducting said sample from said tube to said outlet.

'7. A sampling apparatus for a flowing well having a now control assembly mounted upon and in communication with its bore including, a tubular body adapted to be connected to the control assembly so as to communicate with the well tubing and having a cylinder formed therein, the cylinder having a valve controlled outlet, a piston member slidably mounted within said cylinder, a tube depending from the member and projecting through the lower end of the cylinder into the bore of the body and adapted to be lowered into and raised from the bore of the tubing by said member for receiving a well uid sample, means for sealing oi between the tube and said body bore to prevent direct communication between said cylinder and tubing. a conduit for establishing communication between said tubing and the upper and lower ends of the cylinder, two-way valves for controlling er ends of the cylinder, said member having an annular passage therein communicating with the tube and closed oi by the cylinder wall to prevent the escape of the fluid sample, the passage oi the member registering with the outlet of said cylinder, only when said member is moved to its lower position for conducting said sample from said tube to said outlet.

8. A sampling aparatus for a flowing well having a ow control assembly mounted upon and in communication with the bore of its tubing including, a tubular body adapted to be connected to the control assembly so as to communicate with the bore of the tubing and having a cylinder formed therein, a plunger slidably mounted within the cylinder, means for conducting the well iiuids to and releasing the same from said cylinder for reciprocating the plunger, a. tube depending from said plunger and extending through the lower end of the cylinder into the bore of the body so as to be lowered into` and raised out of the tubing bore upon reciprocation of the plunger, the tube being of suilicient length to extend below the flow connections of said control assembly when lowered by said plunger for obtaining a representative sample of said well fluids, and means for sealing off between said tube and said body bore to prevent direct communication between said cylinder and tubing bore, the body having a discharge port, the plunger having means for establishing communication between the bore of the tube and the discharge port when said tube is lowered into the tubing bore whereby the sample obtained by the tube may be discharged therefrom.

9. A sampling apparatus as set forth in claim 8 wherein the discharge port of the body is formed in the wall of the cylinder, the means of the plunger for establishing communication between the bore of the tube and said discharge port consisting of an angular duct constantly in communication with said tube bore.

HENRY U. JARREI'I. 

